Choline Dihydrogen Phosphate Synthesis Essay

Abstract

Ln 3+-doped (Ln=Sm, Eu, Tb, Dy) nanoparticles of BiPO 4 with a particle size below 10 nm were synthesized in a straightforward manner from the appropriate mixture of the respective metal acetates and the task-specific ionic liquids choline or butylammonium dihydrogen-phosphate by conversion in a laboratory microwave (120 °C, 10 min). The ionic liquid acts not only as a solvent and microwave susceptor, but also as the reaction partner and nanoparticle stabilizer. The materials were thoroughly characterized not only with respect to their optical properties but also by PXRD, FT-IR, TEM techniques. Furthermore, depending on the lanthanide, the nanomaterial shows intense luminescence of different colors such as: orange (Sm 3+), red (Eu 3+), green (Tb 3+) or even white (Dy 3+).

Authors:
Cybinska, Joanna [1]; Lorbeer, Chantal [2]; Mudring, Anja -Verena [3]
  1. Univ. of Wroclaw, Wroclaw (Poland)
  2. Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States)
  3. Iowa State Univ., Ames, IA (United States); Ames Lab., Ames, IA (United States)
Publication Date:
Research Org.:
Ames Lab., Ames, IA (United States)
Sponsoring Org.:
USDOE Office of Energy Efficiency and Renewable Energy (EERE)
OSTI Identifier:
1239836
Report Number(s):
IS-J-8923
Journal ID: ISSN 0022-2313; PII: S0022231315003695
Grant/Contract Number:
AC02-07CH11358
Resource Type:
Journal Article: Accepted Manuscript
Journal Name:
Journal of Luminescence
Additional Journal Information:
Journal Volume: 170; Journal Issue: P2; Journal ID: ISSN 0022-2313
Publisher:
Elsevier
Country of Publication:
United States
Language:
English
Subject:
77 NANOSCIENCE AND NANOTECHNOLOGY; ionic liquid; lanthanides; nanomaterials; luminescence; optical materials; synthesis

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